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Journal : Indonesian Journal of Chemical Research

PRODUKSI DAG DARI VIRGIN COCONUT OIL (VCO) MELALUI REAKSI TRANS-ESTERIFIKASI MENGGUNAKAN ENZIM LIPASE DEDAK PADI (ORYZA SATIVA L.) SPESIFIK C18-20 TERIMOBILISASI KARBON AKTIF SEBAGAI BIOKATALIS Dali, Seniwati; Firdaus, Firdaus; J. Rusman, Hendra
Indonesian Journal of Chemical Research Vol 5 No 1 (2017): Edisi Bulan Juli (Edition For July)
Publisher : Chemistry Department, Pattimura University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598//ijcr.2017.5-sen

Abstract

This research aims to produce DAG of the VCO through the substrate reaction of trans-esterification using lipase enzymes specifically C18-20 from rice bran (Oryza Sativa L.) immobiled of activated carbon as a catalyst. Phases of this research starts with the enzyme lipase do immobile using activated carbon; next enzymes of immobile used to produce DAG through the trans-esterification reaction using a VCO as a substrate and methanol as ko-substrate; DAG and methyl ester produced identified using FTIR instrument and GC-MS instruments. The results showed that there were three compounds DAG and three compound methyl ester produced trans-esterification reaction, namely (1) 1-laurin, 3-heksanoin esters of glycerol; (2) 2-laurin, 3-oktanoin esters of glycerol; (3) 1-laurin, 3-heksanoin esters of glycerol; (4) methyl ester oleic; (5) methyl ester stearic acids; and (6) methyl ester arachidat.
POTENSI EKSTRAK METANOL KULIT BATANG LANNEA COROMANDELICA (HOUTT.) MERR. TERHADAP STAPHYLOCOCCUS AUREUS DAN ANALISIS METABOLIT SEKUNDER UTAMANYANYA Syamsurya, Syamsurya; Ahmad, Ahyar; Firdaus, Firdaus
Indonesian Journal of Chemical Research Vol 4 No 1 (2016): Edisi Bulan Juli (Edition For July)
Publisher : Chemistry Department, Pattimura University

Show Abstract | Download Original | Original Source | Check in Google Scholar

Abstract

This study aims to determine the potential of the methanol extract of the stem bark Lannea coromandelica (Houtt.) Merr. against Staphylococcus aureus and to analyze the main secondary metabolites. Staphylococcus aureus antibacterial activity test was performed by Mueller-Hinton agar medium whereas the secondary metabolite analysis of the methanol extract of the stem bark is conducted by GC-MS instrument. Results of research the methanol extract of bark Lannea coromandelica (Houtt.) Merr showed antibacterial activity against Staphylococcus aureus with inhibition zone diameter each at a concentration of 2.5% by 7.3 mm by 8.6 mm 5% and 10% of 10.4 mm. Selanjunya result of analysis by using GC-MS showed the presence of compounds 5-hidroksimetilfurfural and compounds 1, 2, 3-benzenetriol potential as an antibacterial Staphylococcus aureus. Furthermore, the results of analysis by GC-MS instrumeny showed the presence of compounds 5-hidroksimetilfurfural and compounds 1, 2, 3-benzenetriol potential as an antibacterial Staphylococcus aureus.  
Imobilisasi Enzim Lipase Dedak Padi (Oryza Sativa L.) Pada Karbon Aktif: Karakterisasi, dan Uji Stabilitas Kerja Enzim Imobil Firdaus, Firdaus; Dali, Seniwati; Rusman, Hendra J.
Indo. J. Chem. Res. Vol 5 No 1 (2017): Edisi Bulan Juli (Edition For July)
Publisher : Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (332.428 KB) | DOI: 10.30598//ijcr.2017.5-fir

Abstract

This research aims to immobilization; characterize the enzyme of immobilized, test the effectiveness of the enzyme of immobilized. This research begins with the immobilization to process of enzyme lipase using activated carbon matrix, enzyme characterization covering of immobile determination of temperature and pH optimum of the enzyme of immobilized, as well as test the stability of work covering immobilized of enzyme the test thermal stability and repeated use. The results showed that the immobile of enzyme work optimally at 50oC of temperature and pH 6.5 with each activity 0.040 U/mL; research results also showed that the immobile of enzyme has higher thermal stability in comparison with the free enzyme: with the relative activity of 57.50% at the time of 45 minutes of exposure and the exposure time at 47.50% at 75-105 minutes and it can be used as many as six times with the relative activity of 52.5% in 6 times of use.
SINTESIS SENYAWA N-FENETIL 4-O-ASETIL FERULAMIDA DARI ASAM FERULAT MELALUI REAKSI AMIDASI TIDAK LANGSUNG Fajar Islam, Muhammad; Firdaus, Firdaus; H. Soekamto, Nunuk
Indonesian Journal of Chemical Research Vol 4 No 1 (2016): Edisi Bulan Juli (Edition For July)
Publisher : Chemistry Department, Pattimura University

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Abstract

Compound N-phenetyl 4-O-asetil ferulamide had been synthesized from ferulic acid and phenetylamine through esterification and indirect amidation method. Esterification reaction of ferulic acid with anhydride acetate was done in pyridine solvent at room temperature. Indirect amidation was perform by chlorination using tionyl chloride in benzene solvent at 70°C and continued by amidation with phenetylamine, catalyzed by pyridine in dichloromethane solvent at room temperature. the compound obtained is brown yellowish crystal with melting point 118-120°C. The rendemen of target compound is 53.81%.
SINTESIS TURUNAN AMIDA N-4-O-ASETILFERULOILMORFOLINA DARI ASAM FERULAT MELALUI METODE KONVERSI TIDAK LANGSUNG Sumarna, Sabir; Firdaus, Firdaus; H. Soekamto, Nunuk
Indonesian Journal of Chemical Research Vol 4 No 1 (2016): Edisi Bulan Juli (Edition For July)
Publisher : Chemistry Department, Pattimura University

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Abstract

Synthesis of N-4-O-asetilferuloylmorpholine from ferulic acid via indirect conversion methods with acetylation, chlorination and amidation (in situ) reactions have been conducted. The acetylation was carried out using acetic anhydride reagent in pyridine solvent at room temperature for 6 hours. The chlorination was performed with thionyl chloride in benzene solvent by reflux at 75°C for 4 hours, proceeded by in situ amidation utilizing morpholine in the presence of triethylamine and pyridine using dichloromethane solvent at room temperature. The target molecule as white crystalline solids with m.p. of 91-92°C. Characterization of these compounds was committed by FTIR spectrophotometry.  
ANALISIS KUALITAS MADU MALLAWA BERDASARKAN PARAMETER FISIKA KIMIA Sukmawati, Sukmawati; Noor, Alfian; Firdaus, Firdaus
Indonesian Journal of Chemical Research Vol 3 No 1 (2015): Edisi Bulan Juli (Edition For July)
Publisher : Chemistry Department, Pattimura University

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Abstract

Analysis of chemical physics parameters on Mallawa honey has been done as density, viscosity, HMF, reducing sugars, sucrose and enzyme diastase. The results obtained showed that the average weight of honey Mallawa is 1.373 g / mL, the viscosity of 10.9651 P, HMF amounted to 49.120 mg / Kg, reducing sugar amounted to 70.752% w/w, sucrose at 3:25 w/w and enzymes diastase of 3.805 DN, This is according with ISO and IHC (International Honey Commition) that category Honey Mallawa still good enough for consumption.
Sintesis Turunan Amida N-4-O-Asetilferuloilmorfolina dari Asam Ferulat Melalui Metode Konversi Tidak Langsung Sumarna, Sabir; Firdaus, Firdaus; Soekamto, Nunuk H.
Indo. J. Chem. Res. Vol 4 No 1 (2016): Edisi Bulan Juli (Edition For July)
Publisher : Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (275.249 KB)

Abstract

Synthesis of N-4-O-asetilferuloylmorpholine from ferulic acid via indirect conversion methods with acetylation, chlorination and amidation (in situ) reactions have been conducted. The acetylation was carried out using acetic anhydride reagent in pyridine solvent at room temperature for 6 hours. The chlorination was performed with thionyl chloride in benzene solvent by reflux at 75°C for 4 hours, proceeded by in situ amidation utilizing morpholine in the presence of triethylamine and pyridine using dichloromethane solvent at room temperature. The target molecule as white crystalline solids with m.p. of 91-92°C. Characterization of these compounds was committed by FTIR spectrophotometry.
Potensi Ekstrak Metanol Kulit Batang Lannea coromandelica (Houtt.) Merr. Terhadap Staphylococcus aureus Dan Analisis Metabolit Sekunder Utamanyanya Syamsurya, Syamsurya; Ahmad, Ahyar; Firdaus, Firdaus
Indo. J. Chem. Res. Vol 4 No 1 (2016): Edisi Bulan Juli (Edition For July)
Publisher : Jurusan Kimia, Fakultas Matematika dan Ilmu Pengetahuan Alam, Universitas Pattimura

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (246.338 KB)

Abstract

This study aims to determine the potential of the methanol extract of the stem bark Lannea coromandelica (Houtt.) Merr. against Staphylococcus aureus and to analyze the main secondary metabolites. Staphylococcus aureus antibacterial activity test was performed by Mueller-Hinton agar medium whereas the secondary metabolite analysis of the methanol extract of the stem bark is conducted by GC-MS instrument. Results of research the methanol extract of bark Lannea coromandelica (Houtt.) Merr showed antibacterial activity against Staphylococcus aureus with inhibition zone diameter each at a concentration of 2.5% by 7.3 mm by 8.6 mm 5% and 10% of 10.4 mm. Selanjunya result of analysis by using GC-MS showed the presence of compounds 5-hidroksimetilfurfural and compounds 1, 2, 3-benzenetriol potential as an antibacterial Staphylococcus aureus. Furthermore, the results of analysis by GC-MS instrumeny showed the presence of compounds 5-hidroksimetilfurfural and compounds 1, 2, 3-benzenetriol potential as an antibacterial Staphylococcus aureus.
PREPARASI DAN KARAKTERISASI NI-MO/MONMORILLONIT SEBAGAI KATALIS PADA PROSES CRACKING Sopiarini, Putri; Taba, Paulina; Firdaus, Firdaus
Indonesian Journal of Chemical Research Vol 3 No 1 (2015): Edisi Bulan Juli (Edition For July)
Publisher : Chemistry Department, Pattimura University

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Abstract

This research is aims to prepare and characterization of montmorillonite intercalated Ni-Mo as a catalyst in the cracking process. Preparation is do by extracting monmorillonite of bentonite by decantation method. Monmorillonite synthesized with NaCl to obtain Na-monmorillonite. Ni-Mo/monmorillonite obtained by dissolving ammonium hepta molybdate (NH4)6Mo7O24.4H2O) with distilled water and refluxed with Na-monmorillonite for 6 hours and dried at a temperature of 120oC. Furthermore, nickel nitrate hexahydrate (Ni(NO3)2.6H2O) is dissolved in distilled water and refluxed with Mo-monmorillonite for 6 hours and dried at a temperature of 120oC. Ni-Mo/monmorillonite obtained is then calcined at a temperature of 600oC for 4 hours to activate and eliminate the remnants of organic materials. Characterization of Ni-Mo/monmorillonite do by XRD, XRF and SEM. Characterization by XRD showing the change in the content of monmorillonite, Na-monmorillonite, and Ni-Mo/monmorillonite. Characterization by XRF confirms the success of the creators do with increasing metal content of Ni and Mo in monmorillonite replace the position of the metal Na. Characterization by SEM showed highly significant differences in morphology of montmorillonite, Na-monmorillonite and Ni-Mo-monmorillonite.
UJI FITOKIMIA DAN TOKSISITAS EKSTRAK ETIL ASETAT KULIT BATANG MELOCHIA UMBELLATA (HOUTT) STAPF. VAR. VISENIA DENGAN METODE BRINE SHIRMP LETHALITY TEST (BSLT) Ahmad, Fauziah; H. Soekamto, Nunuk; Firdaus, Firdaus
Indonesian Journal of Chemical Research Vol 4 No 2 (2017): Edisi Bulan Januari (Edition For January)
Publisher : Chemistry Department, Pattimura University

Show Abstract | Download Original | Original Source | Check in Google Scholar | DOI: 10.30598//ijcr.2017.4-fau

Abstract

Melochia umbellata (Houtt) Stapf. var. Visenia is plant species included in Malvaceae family. This spesies is known as paliasa and used as traditional medicine by the people of South Sulawesi. This study aimed to determine the secondary metabolites by reagents and toxicity characteristic testing from bark extract of Melochia umbellata (Houtt) Stapf. var. Visenia using Brine Shirmp Lethality Test (BSLT) method. The extract was prepeared by maceration ethyl acetate. Phytochemical test result showed that the ethyl acetate extract was containing the steroid compound, alkaloids and terpenoids. Toxicity test performed by shrimp Artemia salina Leach larvae was at 48 hours. The toxic effects of the extract were identified by the percentage of the number of shrimp larvae mortality using probit value analysis (LC50). The toxicity test of bark Melochia umbellata (Houtt) Stapf. var. Visenia extract showed that the ethyl acetate extract is toxic to A. salina  LC50 = 54,55 mg / mL.
Co-Authors A. M, Wita Trisnawati Abd. Qohar, Abd. Abd. Wahid Wahab Abdul Kadir Abdul Karim Abdul Kodir Jailani Abdul Razak Abubakar, Achmad Ade Octavia Ade saputra Adelina, Cindi Aeni HM, Nur Aeni HM, Nur Afrian, Noza Afrizon, Hergo Ahmad Muchlis Ahmad Rifai Ahmad Zarkasi Ahmad, Afandi Ahmad, Fauziah Ahmad, Fauziah Ahyar Ahmad Ainul Mardiah Ainunnisa, Ainunnisa Akhyar Akhyar Alfian Noor Alfian Rusdy Ali, Nurhalim Dani Almira Syifa, Almira Amir Hamzah Amnesty, Mulya Fitria Amran Amran Andi Thahir Andini Hardiningrum Anggraini, Rr. Renny Ani Saturrrohmah, Ani Anindia Putri, Riska Anita Desiani Anita Rahayu Anni Faridah Apmayuda, Andrian Aqmal, Amal Ardianto Ardianto Ardiyansyah Ardiyansyah Arifin, Indra Asfar Muniir, Asfar Asgaf, Khaifah Asmawati Asmawati Asrori, Hudi Astari, Lola Astuti, Erni Tri Asyari, Rifa Atul Izza Asyari, Rifa Atul Izza Ayana, Sandy Bakti Azwar, Zainal Bahja, Bahja Bahja, Bahja Bakry Bakry, Bakry Bambang Sujatmoko Bambang Tutuko Bariyah, Naim Buchari, Muhammad Ali Budi Rahmadya Budiyarti, Oky Bustamam Bustamam Bustani, Bustani Dali, Nasriadi Darmansyah Darmansyah Darmawahyuni, Annisa Darussalam Darussalam, Darussalam Dasrol, Dasrol Davit Rahmadan Denas Symond Derisma Derisma, Derisma Dewi, Fatma Dian Anggraini Oktavia Dian Kurnia Anggreta Dian Yayan Sukma, Dian Yayan Dika Sofila Dirgantara, Wahyu Dona Efinda Drs. Helfia MT. Edial Duskiardi Duskiardi Dwi Siswanta Edy Ervianto Efa Ismardianita, Efa Effendi, Sairul Efri Diah Utami, Efri Diah Eka Indarto, Eka Ekardo, Apando Eko s, Randi Wahyu Elfitri, Triana Eli Trisnowati, Eli Era Zulmi Khairani Erdianto Erdianto Erianjoni Erianjoni Erni Haryanti Erwinda Erwinda Ery Safrianti Euis Sunarti Ewaldo, Ivan Ryian Fadilla, Aldy Fadillah, Rahmat Fahrurozi, Fahrurozi Faishal Yasin Fajar Islam, Muhammad Fajri, Bayu Ramadhani Farida Farida Farqi, Muhammad Fatthaya, Fatthaya Fauzan Misra Fauzi Fauzi Febby Asteriani, Febby Febrizal, Febrizal Feranita Feranita Ferawati Ferawati Ferdyan Andhika Pradana, Ferdyan Andhika Fitri, Sri Fitriyanti Jumaetri Sami, Fitriyanti Jumaetri Fitriyanto, Aidil Fri Murdiya, Fri Galib, Muhammad Ganefri Ganefri Gaol, Dedek S Lumban Ginting, Bayudwi Putra Gita Hermi Setyawati H. Soekamto, Nunuk Hadria Octavia Handayani, Endah Harahap, Heri Faisal Hardjono Sastrohamidjojo Hariani Soekamto, Nunuk Harifuddin Harifuddin, Harifuddin Harison, Torang hasan, effendi Hasnah Hasnah Hasnah Natsir Hayatul Ismi Hendra Naldi Hendra Setiawan Hendri Marhadi Hendri, Ulfa Nurhasanah Hersyah, Mohammad Hafiz Hesti Meilina Hidayat, Reski HIDAYATULLAH, ARIEF Huda Ubaya Husni Husni Idral Purnakarya Ifwandi Ifwandi, Ifwandi Ihsan, Akmal Ilahi, Yudhi Fasrah Imma Fretisari Indrasari, Rahmayani Irfan Hamdani, Irfan Irma Yanti Irwani, Nike Ishak Erawadi Barutu, Ishak Erawadi Iskandar Zulkarnain Islam, Muhammad Fajar Ismail Ismail Ismail Kailani, Ismail Ismail Suardi Wekke Ismala, Silvi Iswani, Resti J. Rusman, Hendra Jalifah Latip Johari, Rizky Jumina Jumina Juneidi, Ahmad Kaharuddin Kaharuddin Kamariyah, Nurul Karmin Karmin, Karmin Katrin Roosita Khairani Khairani Khuzaini, Khuzaini Kolo, La Komariah, Sita Kurniati Asri Kurniawan Kurniawan Lestarini, Dinda Lewi Lewi Lifwarda Lifwarda Linna Oktaviana Sari Lintang, Elba Lubis, Citra Rahmawati Lubis, Putri Mirta Fitriyanti Lukman Hakim Lusiana, Herlina Lusiana, Herlina Lysbetti M, Noveri M Aldion Rinaldi, M Aldion M Putra Nurjanah, M Putra M, M. Dahlan M, Noveri L M. Dani M. Muafif, M. Muafif Maihasni Maihasni Maiyendra, Nico Alvio Maming Maming Mardiah, Indah Martadinata, A. Taqwa martati, Eli Martha, Cici Wia Maryati Bachtiar Mawaddah Warahmah Md. Nor Bin Bakar, Md. Nor Bin Medilla Kusriyanto, Medilla Meza Silvana Michael, Donny Miftah Azrin Miftahul, Hendri Minsyah, Nur Imdah Mira Afrina Miraswan, Kanda Januar Mirza, T. Mohd Mohd Yogi Yusuf, Mohd Yogi Muafif, M Mubaraq, Fitratul Muchlis Djirimu Muhamad Al Khausar, Muhamad Al MUHAMMAD ANSHORI, MUHAMMAD Muhammad Arif Muhammad Fathra Fahasta Muhammad Ibrahim Muhammad Isya Muhammad Nur Muhammad Sayuthi MUHAMMAD SHOLEH Mulyani, Pamungkas Stiya Nafis, Muhammad Nafliana, Ela Aprida Nalom Kurniawan Nani Nani Nasir, M Iqbal Nawas, Kamaluddin Abu Nesya, Hamidatul Netti Herawati Nilda Elfemi Nindya, Audesti Nota Effiandi Novesar Jamarun Nugraha, Rendy Dartha Nunuk H. Soekamto Nunuk Hariani Soekamto Nur Ahriman, Nur Nur, Hanis Nurcahyani, ida Nurcahyani, ida Nurhalim Nurhalim, Nurhalim Nurhasanah Nurhasanah Nurhayati Nurhayati Nurmilasari, Nurmilasari Nurus Shalihin, Nurus Oktisari, Dwi Orsalan, Osvari P., Elman Paly, Muh Basir Pascawinata, Andries Paulina Taba Periyadi, Periyadi Prasetya, Dwi Arman Prasetya, Febri Prima, Prima Purnama, Azet Putra, Ario Putra, Ozil Afindra Putri, Adi Tiara Rachmatullah, Muhammad Naufal Rahmat Saleh Rahmawati Rahmawati Rahmi Holinesti Rahmi Widyanti Rahmon Sandika Rahmat, Rahmon Sandika Rahmy, Hafifatul Auliya Rahyul Amri Rakiman Rakiman Ramadhan, Waldito Febri Ramadhani, Anissa Ramadhani, Anissa Ranuharja, Fadhli Ratna Aisuwarya, Ratna Ratna Dewi Retnaningsih Retnaningsih Reza Al Mattin, Reza Al Rhozi, Fahrul Rifqi Muntaqo, Rifqi Rikki Vitria Rimbawan Rimbawan Rinel Fitlayeni Riska Fitriani Rita Hayati Rizal Amin, Muhammad Rodiah, Desty Romli Romli, Romli Rusdarti Rusdarti, Rusdarti Rusman, Hendra J. Sabran, Moh. Sagala, Alberto Syahputra Saifuddin Saifuddin Salmiyah, Salmiyah Salvia Salvia Sandi Firman Nanda, Sandi Firman Sani, Almadora Anwar Sano, Havel Alindo Santy, Wesiana Heris Saprianto, Saprianto Sari, Firda Mustika Sari, Rahayu Eka sari, sally nindi Saribu, Daniel Harjono Dolok Sarifah Putri Raflesia, Sarifah Putri Saripah Ulpah, Saripah Sarjon Defit Sarmayanta Sembiring Seniwati Dali Septianto, Dekri Sibarani, Hendri Agustin Sigit Sutikno, Sigit Silfia Rifka Sitanggang, Miranda Romaully Br. Siti Hafsah Siti Nurmaini Soejono Tjitro Sofiarsih, Lilis Solehan, Muhamad Somakim Somakim Sopiarini, Putri Sopiarini, Putri Sri Anna Marliyati Sri Indra Maiyanti Stevany, Cecilia Suana, Suana Sudardi, Sudardi Sudarmantoro, Niky Suharyon, Suharyon Sukim, Sukim Sukmawati Sukmawati Sulfasyah Sulfasyah, Sulfasyah Sulistioso G. S. Sulkifli Sulkifli Sumarna, Sabir Sumarna, Sabir Sunardi Sunardi Surya Prahara Surya Setiawan, Surya Suryadi Suryadi Susanki Susanki Sutrisno sutrisno Syafniati, Syafniati Syahrilfuddin Syahrilfuddin, Syahrilfuddin Syakban Kurniawan, Syakban Syam, Jumriah Syamsuddin Syamsuddin Syamsurya, Syamsurya Syamsurya, Syamsurya Syarifah Syarifah, Syarifah Tati Erlina Taufik Ahmad Thamrin Thamrin Tjut Chamzurni Tri Suminar Tumpak Dolok Stepan Simarmata, Tumpak Dolok Stepan Tuti Handayani, Tuti Tuti Handayani2, Tuti Tuti Restuastuti Tutri, Rio Ulfia Hasanah Umamah, Farida Upasana Narang, Upasana Usman, Regina Utami, Annisa Desria Wagiyo Wagiyo Wahyu, Arbi Wahyudi Budi Pramono, Wahyudi Budi wahyuni wahyuni Wahyuni, Dinar H S Wahyuni, Ritna Warasto, Hestu Nugroho Warman, Ari Gustia Wilyanto, Wilyanto Wilyanto, Wilyanto Winaldi, Aulia Winner Inra Jefferson Batubara, Winner Inra Jefferson Wullur, Selfi Yandi, Satria Yasin, Haerun Yeni Wulandari Yolanda, Sri Yani Yuanto, Dedy Ary Yul Antonisfia Yuli Yetri Yulindon Yulindon Yulisa, Ike Yunus, A.M Shiddiq Yunus, Yuhanis Yustini Yustini Yusuf Hartono Yusuf Ridho Surya Dharma Nainggolan, Yusuf Ridho Surya Dharma Zabidi, Ahmad Zainal Arifin Zainal, Syech Zohra Hasyim, Zohra Zulfiadi, Zulfiadi Zulharbi Zulharbi Zusmelia Zusmelia Zuyasna Zuyasna